Magnetic field induced orientation of superconducting MgB${}_2$ crystallites determined by X-ray diffraction

Abstract

X-ray diffraction studies of fine polycrystalline samples of MgB${}_2$ in the superconducting state reveal that crystals orient with their \emph{c}-axis in a plane normal to the direction of the applied magnetic field. The MgB${}_2$ samples were thoroughly ground to obtain average grain size 5 - 10 $\hat{I}¼$m in order to increase the population of free single crystal grains in the powder. By monitoring Bragg reflections in a plane normal to an applied magnetic field we find that the powder is textured with significantly stronger (\emph{0,0,l}) reflections in comparison to (\emph{h,k,0}), which remain essentially unchanged. The orientation of the crystals with the \emph{ab}-plane parallel to the magnetic field at all temperatures below $T_c$ demonstrates that the sign of the torque under magnetic field does not alter, in disagreement with current theoretical predictions.